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采用溶胶-凝胶法在多孔氧化铝模板上制备立方相WO3纳米线
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Sol-Gel Derived Cubic-Phase WO3 Nanowires on Nano- Porous Alumina Template
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National “973” Project (2007CB936601); National Natural Science Foundation (50872064) of China; Knowledge Innovation Project of Chinese Academy of Sciences (KGCX2-YW-341); China Postdoctoral Science Foundation (20090450581); K. C. Wong Education Foundation , Hong Kong

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    摘要:

    采用溶胶-凝胶法在纳米孔氧化铝模板上成功制备形貌各异的WO3纳米线。X射线衍射分析表明所制备的WO3纳米线为立方相结构。经扫描电子显微镜观察发现产物多数为菊花状WO3纳米线,其直径约10~80 nm,长约几微米。与空气气氛相比,氩气气氛更有助于WCl6三嵌段共聚物溶胶在多孔氧化铝模板上形成形貌各异的WO3纳米线。

    Abstract:

    WO3 nanowires with various morphologies were prepared on nanoporous alumina template by a simple sol-gel method. X-ray diffraction analysis reveals that the obtained materials are cubic WO3. Scanning electron microscopy shows that the products contain chrysanthemum-shaped WO3 nanowires. The diameter of WO3 nanowires is about 10-80 nm and their length is up to several micrometers. Argon gas atmosphere is more favorable for WCl6-triblock copolymer sol to form WO3 nanowires with different morphologies on nanoporous alumina template than air atmosphere.

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徐宇兴,谭强强,唐子龙,张中太,袁章福.采用溶胶-凝胶法在多孔氧化铝模板上制备立方相WO3纳米线[J].稀有金属材料与工程,2010,39(5):753~755.[Xu Yuxing, Tan Qiangqiang, Tang Zilong, Zhang Zhongtai, Yuan Zhangfu. Sol-Gel Derived Cubic-Phase WO3 Nanowires on Nano- Porous Alumina Template[J]. Rare Metal Materials and Engineering,2010,39(5):753~755.]
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  • 收稿日期:2009-05-17
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