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氧化钛纳米管阵列热驱动掺银及其生物活性和抗菌性研究
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西北工业大学凝固技术国家重点实验室,中国兵器科学研究院宁波分院,中国兵器科学研究院宁波分院,中国兵器科学研究院宁波分院,包头医学院第一附属医院

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浙江省科技计划项目 (No 2013C31051)


Titania nanotube arrays thermal drive Ag doped and its bioactivity and antibacterial performance
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State Key Laboratory of Solidification Processing,Northwestern Polytechnical University,Ningbo Branch of China Academy of Ordnance Science,Ningbo Branch of China Academy of Ordnance Science,Ningbo Branch of China Academy of Ordnance Science,The First Affiliated Hospital of Baotou Medical College,Baotou,Inner Mongolia

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    摘要:

    本文通过在纯钛表面制备得到氧化钛纳米管阵列后,再利用热驱动掺银技术,成功制备得到既具有生物活性,又具有抗菌性能的银掺杂氧化钛纳米管阵列。研究表明氧化钛纳米管阵列热驱动掺银的机理为硝酸银在受限反应空间中的低温分解及其与氧化钛低温相变的协同。将氧化钛纳米管阵列浸泡饱和硝酸银后,在300℃条件下热处理,不仅能实现氧化钛纳米管阵列由无定型转变为金红石型的低温相变,还能同时实现硝酸银的低温分解。

    Abstract:

    In this paper, the Ag-doped titania nanotube arrays was successfully fabricated by steps of preparation of titania nanotube arrays on the surface of pure titania and the Ag-doped technology of thermal drive, which has excellent bioactive and antibacterial performance. The researches show that the mechanism of thermal drive Ag-doped is the collaboration of thermal decomposition of silver nitrate in the limited space with the phase transition of titania at low temperature. After being soaked in saturated silver nitrate and annealed at 300℃, the titania nanotube arrays can realize not only the low temperature phase transition from amorphous to rutile, but also the low temperature decomposition of silver nitrate within it.

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田甜,顾明俊,董海成,马兰,胡同平.氧化钛纳米管阵列热驱动掺银及其生物活性和抗菌性研究[J].稀有金属材料与工程,2017,46(4):1020~1025.[Tian Tian, Gu Mingjun, Dong Haicheng, Ma Lan, Hu Tongpin. Titania nanotube arrays thermal drive Ag doped and its bioactivity and antibacterial performance[J]. Rare Metal Materials and Engineering,2017,46(4):1020~1025.]
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历史
  • 收稿日期:2014-12-16
  • 最后修改日期:2015-02-06
  • 录用日期:2015-03-25
  • 在线发布日期: 2017-08-04
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