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Ti活度对Al2O3/AgCuTi/Fe-Ni-Co钎焊接头机械性能和微观组织结构的影响
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四川大学制造科学与工程学院,四川大学制造科学与工程学院,四川大学制造科学与工程学院,四川大学制造科学与工程学院,四川大学

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航空科学基金资助(20100119003)


Effects of Ti Activity on Mechanical Performance and Microstructure of Al2O3/AgCuTi/Fe-Ni-Co Brazed Joints
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Sichuan University,,,,

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    摘要:

    采用AgCuTi钎料实现了Al2O3陶瓷与Fe-Co-Ni合金的钎焊连接,并调查了不同钛含量的钎料对Al2O3/AgCuTi/Fe-Ni-Co钎焊接头机械性能和微观组织结构的影响。扫描电子显微镜(SEM), X射线能量色散光谱仪(EDS), X射线衍射仪(XRD)及电子万能试验机用于分析钎焊接头的机械性能和微观组织结构,结果表明:钛含量的增加明显提高AgCuTi钎料与Al2O3陶瓷的相互作用,在Al2O3/Ag-Cu-Ti界面生成一层由Ti-Al 和 Ti-O化合物组成的反应层。Al2O3/AgCuTi/Fe-Ni-Co钎焊接头的抗拉强度随钛含量的增加而增加,当钛含量提高到8wt.%时,抗拉强度达到最大值78Mpa。通过微观组织结构分析发现,采用AgCu4Ti在890℃保温5min的条件下可以获得较好的钎焊接头,典型接头的微观组织结构为Al2O3/TiAl+Ti3O5/NiTi+Cu3Ti+Ag(s,s)/Ag(s,s)+Cu(s,s)+(Cu,Ni)/Fe-Ni-Co。采用AgCu8Ti获得的钎焊接头的界面反应层与AgCu4Ti差异不大,但反应层稍微增厚,并伴有TiO和Ti3Al在Al2O3/Ag-Cu-Ti界面生成。

    Abstract:

    Al2O3 ceramic/Fe-Ni-Co joints are achieved using Ag-Cu-Ti filler alloy in the study to investigate the dependence of the joint microstructure and mechanical performance on the Ti content. Scanning electron microscope (SEM), energy dispersive X-Ray spectrometer (EDS), X-Ray diffractometer (XRD) and electronic universal testing machine are used to characterize the microstructure and mechanical performance of the joints. The results show that the increase of Ti content can obviously intensify the interaction between Al2O3 and Ag-Cu-Ti. A layer of Ti-Al and Ti-O products is observed at the interface of Al2O3/AgCuTi. The tensile strength of Al2O3/AgCuTi/Fe-Ni-Co joint increase as the Ti content increased from 2 wt% to 8 wt.%, and the tensile strength of brazing joint reached the maximum value of 78MPa. Good reaction layer formed by metallurgical reaction at the interface of Al2O3/AgCu4Ti, and the typical microstructure is Al2O3/TiAl+Ti3O5/NiTi+Cu3Ti+Ag(s,s)/Ag(s,s)+Cu(s,s)+(Cu,Ni)/Fe-Ni-Co brazed at 890oC for 5 min. Compared with AgCu4Ti filler, the microstructure of the joints change slightly when addition of the active element Ti to 8 wt.% except for the increase of the thickness of reaction layer adjacent to Al2O3 ceramic and accompanied the formation of TiO and Ti3Al in the Al2O3/Ag-Cu-Ti interface.

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辛成来,李宁,颜家振,曹永同,刘文博. Ti活度对Al2O3/AgCuTi/Fe-Ni-Co钎焊接头机械性能和微观组织结构的影响[J].稀有金属材料与工程,2018,47(4):1031~1036.[Xin Chenglai, Li Ning, Yan Jiazhen, Cao Yongtong, Liu Wenbo. Effects of Ti Activity on Mechanical Performance and Microstructure of Al2O3/AgCuTi/Fe-Ni-Co Brazed Joints[J]. Rare Metal Materials and Engineering,2018,47(4):1031~1036.]
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  • 收稿日期:2016-09-02
  • 最后修改日期:2016-10-11
  • 录用日期:2016-10-18
  • 在线发布日期: 2018-05-31
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