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功能梯度 WC-Co/WC-Fe-Ni双层硬质合金的研究
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1.郑州航空工业管理学院;2.中南大学

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Study of the functionally graded WC-Co/WC-Fe-Ni double-layer cemented carbides
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1.Zhengzhou University of Aeronautics;2.Central South University

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    摘要:

    使用新的制备方法成功制备了功能梯度WC-Co/WC-Fe-Ni双层结构硬质合金。冷压成型所需的压制压力需要保持在15 MPa,在这个压力下WC-Co和WC-Fe-Ni层的烧结收缩率相同,制备的双层合金没有分层和裂纹等不利现象出现。采用X射线衍射(XRD)、光学显微镜(OM)和扫描电子显微镜(SEM)等实验手段研究了双层合金的相组成与微观结构,发现合金中没有η或者石墨相的存在,而且,WC-Co和WC-Fe-Ni层间的界面处结合良好。同时,在WC-Co/WC-Fe-Ni双层结构硬质合金的界面处有明显的连续变化的 Fe, Ni 和 Co 成分梯度,两层间的成分梯度导致界面附近的硬度梯度的形成。制备的功能梯度WC-Co/WC-Fe-Ni双层结构硬质合金同时高的硬度、耐磨性和韧性。

    Abstract:

    We investigated the properties of functionally graded WC-based cemented carbide, prepared with a new approach featured by sintering the WC-Co/WC-Fe-Ni double-layer compacts together. For this approach, the reasonable pressing pressure to prepare the alloys should be about 15 MPa, under which the two layers have consistent sintering shrinkages and the unexpected phenomena (e.g. layering and cracking) were not observed. The phase composition and microstructure analysis based on the X-ray diffraction, optical and scanning electron microscopy experiments indicate that the η or graphite phase is not existed in both WC-Co and WC-Fe-Ni layers, and that the interface of these two layers are well combined together. Meanwhile, a significant gradient of Fe, Ni and Co is observed at the interface between the above two layers, and this composition gradient results in a noticeable hardness gradient, which further leads to the WC-Co/WC-Fe-Ni double-layer cemented carbide being of high hardness, wear resistance and toughness.

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高阳,罗兵辉,柏振海.功能梯度 WC-Co/WC-Fe-Ni双层硬质合金的研究[J].稀有金属材料与工程,2020,49(3):842~848.[gaoyang, luobinghui, baizhenhai. Study of the functionally graded WC-Co/WC-Fe-Ni double-layer cemented carbides[J]. Rare Metal Materials and Engineering,2020,49(3):842~848.]
DOI:10.12442/j. issn.1002-185X.20181132

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  • 收稿日期:2018-11-12
  • 最后修改日期:2019-02-26
  • 录用日期:2019-03-14
  • 在线发布日期: 2020-04-08
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