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机械合金化制备Fe-Cr-Mn-N奥氏体不锈钢厚熔覆涂层的研究
作者:
作者单位:

1.西安交通大学材料科学与工程学院;2.中国船舶重工集团公司第七二五研究所 海洋腐蚀与防护重点实验室 青岛

基金项目:

海洋腐蚀与防护重点实验室开放研究(项目号6142901180402)


Preparation of Fe-Cr-Mn-N austenitic stainless steel thick cladding coating by mechanical alloying
Author:
Affiliation:

1.School of Materials Science and Engineering,Xi’an Jiaotong University,State Key Laboratory ofMetal Material Strength,Xi’an Shan Xi;2.State Key Laboratory for Marine Corrosion and Protection,Luoyang Ship Material Research Institute LSMRI

Fund Project:

State Key Laboratory for Marine Corrosion and Protection

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    摘要:

    本实验采用机械合金化方法制备了Fe76Cr12Mn12N合金粉末,研究其机械合金化过程,并对机械合金化的机制进行探讨。研究表明,棒磨4小时时粉末就可以完全合金化,并且随着棒磨时间增加,衍射峰逐渐宽化,衍射强度逐渐降低。粉末颗粒形貌也逐渐类球形化。机械合金化得到的非球形固溶体粉末也可用于激光熔化沉积(LMD)增材制造技术,解决了LMD对球形粉末的局限性,机械合金化粉末通过LMD技术得到的厚熔覆涂层具有较好的耐蚀性,其物相结构是BCC+FCC的双相结构,同时在打印过程中有Cr2N生成,维氏硬度最高达到456.3HV。

    Abstract:

    In the experiment, Fe76cr12mn12n alloy powder was prepared by mechanical alloying. The mechanical alloying process and mechanism were studied. The results show that the powder can be fully alloyed after 4 hours of rod milling. The diffraction peak widens and the diffraction intensity decreases with the increase of rod milling time,. The morphology of the powder particles gradually became spherical. The non-spherical solid solution powders obtained by mechanical alloying can also be used in laser melting deposition (LMD) additive manufacturing technology, which solves the limitation of LMD to spherical powder. The thick cladding coating obtained by LMD technology has good corrosion resistance, and it shows BCC+ FCC dual phase structure. Meanwhile, Cr2N is generated in the printing process. the Vickers hardness of thick coating could reach up to 456.3 HV.

    参考文献
    参考文献 References
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高帅龙,孙德福,谷臻,孙崇峰,席生岐,彭文山.机械合金化制备Fe-Cr-Mn-N奥氏体不锈钢厚熔覆涂层的研究[J].稀有金属材料与工程,2022,51(1):321~326.[Gao Shuailong, Sun Defu, Gu Zhen, Sun Chongfeng, Xi Shengqi, Peng Wenshan. Preparation of Fe-Cr-Mn-N austenitic stainless steel thick cladding coating by mechanical alloying[J]. Rare Metal Materials and Engineering,2022,51(1):321~326.]
DOI:10.12442/j. issn.1002-185X.20210075

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  • 收稿日期:2021-01-24
  • 最后修改日期:2021-04-21
  • 录用日期:2021-04-30
  • 在线发布日期: 2022-02-09
  • 出版日期: 2022-01-28