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Structure and Energy Storage Characteristics of Re2O3(Re=Pr, Nd)-Doped SrTiO3 Ceramics
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    Abstract:

    Rare earth oxides Re2O3 (Re=Pr, Nd) doped SrTiO3 ceramics with the formula of [Re0.02Sr0.97(VSr)0.01]TiO3 (Re0.02Sr0.97TiO3: Re-STO) were prepared by a solid state reaction method. The X-ray diffraction (XRD) results indicate that Re-STO ceramics have a single cubic perovskite structure which is similar to that of pure SrTiO3. Scanning electron microscopy (SEM) analysis shows inhomogeneous grain size distribution in Re-STO ceramics with big grains of about 10 μm and small ones of about 1 μm, and the small grains normally exist in grain boundaries and/or triangle grain boundaries among big grains. The dielectric properties of Re-STO ceramics were measured by HP4294 precision impedance analyzer, JJC9906-A breakdown strength testing instrument and FMRL bias voltage testing system, and the energy storage characteristics was evaluated. The results show that the relative dielectric constants of Re-STO ceramics (Pr-STO: εr=1860; Nd-STO: εr=1670), prepared at the optimized sintering temperature of 1350 oC, increase by more than 5 times than that of pure STO ceramics (εr=300 kHz), while the dielectric loss of Re-STO ceramics still remains lower than 0.03 (1 kHz). The breakdown strength Eb of Re-STO ceramics is higher than 15 kV/mm. Under the bias voltage testing conditions used in this study, the εr of Re-STO ceramics changes within ±12%, and the relationship between energy storage density and bias voltage is in good line with quadratic parabola function. Therefore, Re-STO ceramics can be treated as linear dielectrics, which should be very promising for medium/high voltage solid state energy storage applications. Meanwhile, the relationship between the phase structure, microstructure, possible defect structure and the dielectric properties, energy storage characteristics of Re-STO ceramics were also discussed.

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[Shen Zongyang, Hu Qiguo, Li Yueming, Wang Zhumei, Luo Wenqin, Hong Yan, Xie Zhixiang, Hong Lu. Structure and Energy Storage Characteristics of Re2O3(Re=Pr, Nd)-Doped SrTiO3 Ceramics[J]. Rare Metal Materials and Engineering,2014,43(7):1671~1675.]
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History
  • Received:July 28,2013
  • Revised:
  • Adopted:
  • Online: December 15,2014
  • Published: