Kaug Xinting , Jiang Jiling , Liu Shuying
1995(1).
Abstract:brief introduction is presented for the methods of corn bustion synthesizing TiN including gas-solid,liquid-solid, and solid-solid methods.The effective factors of all these methods are also-discussed in detail. The results show that solid-solid methos is insensitive to nitrogen pressure and diluent,it is one of the simplest technology in the three methods.However,the most typical and common method is gas-solid cormbustion synthesizing method,due to the avilable of nitrogen resoursce.
Wan Juling , Gu Jialing , Chen Nanping
1995(1).
Abstract:采用920℃下不同应变速率的压缩实验,较为系统地研究了具有明显的组织定向排列的Ti6Al4V合金非等轴组织的应力应变关系、应力应变速率关系及应变速率敏感性随应变的变化,实验发现在组织取向与应力轴方向之间的夹角不同的情况下,上述各关系具有不同的特征,并从两相变形的特点、变形中的晶粒转动和组织等轴化的角度对实验结果给出了定性的解释。
Wu Qingzhi , Li Zuochen , Wang Weimin
1995(1).
Abstract:研究了氧含量(0.10Wt%~0.30Wt%)对Ti-75合金组织和性能的影响。试验表明,在所研究的范围内,β晶粒长大的速度随氧浓度增加而减小,强度、硬度、电阻线性增加,塑性及显微组织变化不大,冲击值虽显著降低,但当氧达到0.20Wt%时,aK值仍有460kJ·m-2,由此可见,氧控制在0.20wt%以下,可得到综合性能良好的Ti-75合金。
Liu Minghu , An Meiling , Zhang Sijing
1995(1).
Abstract:escribes a new process to produce palladium chloride directly with recover palladium by Zinc-magnesium recovery and mixed acid dissolving fro m waste C - Pd catalyst.Higher recovery of palladium and rapid red notion can be obtained cormpared with conventional aluminium reduction process.
Chu Shuangjie , Hu Keao , Wu Renjie
1995(1):1-6.
Abstract:Introduce the principle of magneto-optical recording and substrate materials of magneto-optical disk, specifically the properties,manufscture methods and protective film of the rare earth-transition metal(RE-TM)alloy amorphous film.And simply describes the properties and feature of oxide single-crystal,multi-crystal and multiple-story magneto-optical recording film. It is pointed out that the future developing tendency will be multi-layes magneto-optical recording materials.
1995(1):15-20.
Abstract:he development and researching situation of silver, titanium and aluminum based brazing filler for Ti and Ti alloys are reviewed. The advantages and disadvantages of them are discussed. The development tendency of brazing filler metals for Ti and Ti alloys is analyzed.
Pang Yunhong , Zhou Yu , Jiang Yi , Zhou Yigang
1995(1):33-37.
Abstract:研究了Ti-6.5Al-3.5Mo-1.5Zr-0.3Si合金细观结构对裂纹扩展特性的影响。发现当△K值小于da/dN-△K曲线上转折点处△K值时,合金出现解理断裂,表明转折点是解理断裂向条纹机制断裂的过渡;大量试验又进而证明,解理断裂与裂尖塑性区大小和裂纹穿过的晶粒或晶域尺寸有关。由此,作者提出了钛合金在裂纹扩展过程中形成解理断裂的一种新的断裂机制。
Wang Jingtao , Wang Haibo , Xu Yuzhong , Pang Yuhua
1995(1):38-42.
Abstract:Dendrite arm spacings of alum inium and Al-Mn, Al-Cu, Al-Li,etc.14 aluminium alloys with minor Rare Elements added have been studied. Present investigation indicates that minor addition of Rare Earth Elements La,Ce or Yobviously refined the dendrite structure of commercial pure aluminium and aluminium alloys.The refining effect of Rare Earth Elements on dendrite arm spacings was directly related to the"quality"and'quantity'of alloying elements in the base alloy,this was reflected by the solute transportation characteristic parameter Po proposed in this paper;The refining effect of Rare Earth Elements on dendrite arm spacings was also related to the cooling rate during solidification. The higher the cooling rate,the weaker the refining effect of Rare Earth Element on dendrite arm spacings.Although some additives were indicated to be very effective in refining grain size of aluminium alloys,their refining effect on dendrite arm spacings were found to be very weak.
1995(1):43-48.
Abstract:利用自蔓延高温合成(SHS)熔铸技术,将碳化铬的高温熔体铺展在平面样品的钢表面上,从而形成厚度为几毫米的熔覆层。为克服碳化铬与底材的润湿问题,采用与Fe有良好互溶性的Cr作为润湿功能层,在此基础上,使Cr-C合金层中的碳作阶梯改变,从而获得了梯度熔覆层结构。来用N2加压(<20MPa)和预热工艺(≤300℃)等措施,控制反应燃烧温度,改善熔体流动性,增大熔渣分离速度,有利于提高熔覆层表面平滑程度。研究认为,良好的结合强度来源于界面间强烈的冶金作用以及梯度成分分布。
He Guiyu , Chu Shuangjie , Hu Shiping
1995(1):49-54.
Abstract:介绍了涂覆Y2O3的Ti纤维增强γ-TiAl基复合材料的研究结果,分析了其界面结构和力学性能特征。试验结果表明,用物理气相沉积法(PVD)在其表面涂覆Y2O3层的Ti纤维增强TiAl基复合材料,不仅使TiAl合金的弯曲强度提高25%,而且在同一工艺条件下使Ti纤维与TiAl基体间的界面反应层厚度由原来的30μm减小到14μm,界面有新相Ti3Al产生。
1995(1):55-60.
Abstract:测定了含Ce0.06wt%及0.15wt%的1420合金板材的时效硬化曲线及室温力学性能,分析了Ce对1420合金时效过程的影响。结果表明:Ce含量在0.15wt%范围内的1420合金时效的组织与不含Ce的1420合金类似,主要强化相为δ'及δ'/β'复合相。微量Ce在1420合金中可以减缓固溶处理时的再结晶过程及细化再结晶晶粒,并促进δ'相在时效过程中的弥散析出。添加0.06Wt%Ce时有利于提高合金塑性,而添加0.15wt%Ce时则有利于提高合金强度。采用465℃固溶,2%预拉伸变形及170℃/6h时
1995(1):64-68.
Abstract:以I3-淀粉配合物为指示剂,用停流FIA光度法研究了钼(VI)和钨(VI)对H2O2-I氧化还原反应体系的协同催化效应,并定义了协同催化系数D以表示这种协同作用的大小。将此系数引入到停流FIA-动力学体系多组份同时测定的方法中,可有效地补偿吸光度对加和性的偏离,并可降低检出限。用本法测定钼(Ⅵ)和钨(Ⅵ)的线性范围分别为0~1.1μg·ml-1和0~2.0μg·ml-1,而未补偿时则分别为0~0.6μg·ml-1和0~0.8μg·ml-1。测定了钢样及模拟样品中的用和钨含量,结果满意。钼、钨的回收率分别为
1995(1):69-74.
Abstract:he corrosion perforative equipment made of titanium used for mash shadow of colour TV has been manufactured successfully for the frist time in china.It has been running stable for two years since it was put into operation.The productivity and qualified products have increased by 10% and 6% respectively.It costs about 15% of that of imported one,therefore is a good alternative for the later.The design and manufacture of this production line have reached international level and open a new field for titanium application.
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